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 the
Hive BB  Crystal
Meth  ok
all ya Li?Nh3 freaks, the last of the trials r bein done...reslts soon!
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| Author | Topic: ok all ya Li?Nh3 freaks, the last of the trials r bein done...reslts soon! |
| mrr
pyrex Worker Bee |
posted 01-05-2000 06:16 AM
Yes, that is correct! If'n ya be sittin on the edge of u'r seats waitin for guidelines well thee wait be soon over! ;-) But CHEMGUY-->e-mail me if'n ya would...would like to make this presentation a co-op project(i.e pyrex/guy) to the hive/Rhodium/////Pyrex@home.com Well get your tooters ready! ;-) Pyrex out |
| Xion NewBee |
posted 01-05-2000 10:36 AM
Ill bite in this one . It would be good to see some solid advances on this one. Even just avanced techniques. Go-Go man!!! |
| Zeph NewBee |
posted 01-05-2000 10:40 AM
Do you think you guys could work together to get the job done? With all that hassing you do each other ? I thought you guys hated each other , well good luck! |
| mrr
pyrex Worker Bee |
posted 01-05-2000 05:44 PM
Well I can't speak for him, but I don't hold nothing against him....yes he may indeed hold something against me, cause yes I did unecessarily harrass him, when he posted before about Li/Nh3, and if'n you do hold anything against me-->I'm sorry for the unneeded responses I gave ya. But I am aware that he is more knowledgable in this field then I am when it comes to facts from the books. What information i'm willing to post is actual tried results, but that kind of post would be lacking the scientific reasoning why it would or wouldn't work, which is why I'm asking him if'n he wants to fill in what I can only guess at. Either way I will still post method, I just figured it might be a better post if'n we put knowledge together, seeing as how it might be good enough for rhodium's board, I wouldn't want to submit stuff that isn't detailed with guidelines that have some factual backing. Anyway I'm rambling. Pyrex out |
| CHEM
GUY Worker Bee |
posted 01-05-2000 07:30 PM
No, I don't hold anything against you mrr pyrex. Almost all of my information is posted now, but if you want a question answered just post it and I will try to answer quickly as possible. Also, I'm sure you are aware of my prefered method of Birch reduction. I prefer to add the alkali metal after the addition of the ephedrine to the NH3 (or whatever compound you use). This way the NH3 need not be anhydrous, which is difficult to acheive, but, depending on the proton donator content, you will need to add more than a 2 to 1 ratio of alkali metal to ephedrine free base. Just glad to help ------------------ |
| mrr
pyrex Worker Bee |
posted 01-07-2000 03:48 AM
Well I'm not saying that I have tried the method you just proposed...but someone recently, very recently observed a dream that followed that idea to a TEE, meaning the condensed NH3 was allowed to gather in the bottom of a 250ml round bottom flask then Gilligan decided to throw in 4gms of freebase(which by the way had no intentions of dissolving in that NH3, even with violent shaking, stirring, nothing), so then the Professor walked in an said hey let me help you there, and he threw in (1)2450 Li cell, immediately deep blue color was noted. The rxn vessel was mixed realll well, by the Skipper for about 3-5mins. Then Mr. Howell came in and threw in about 150mls of Ethyl Ether(sp?), and bang instantly blue went away, then H20 was added by Mary Ann to make sure there was no left over Li in the vessel. Then Mrs. Howell(mrs. KNOW-IT-ALL), said give me that, and she proceeded to gas it, and low and behold a blizzard appeared, HOWEVER when Ginger the TEST monkey tried it....BBBLLAAAHHHH, some of the nastiest crap she had ever been subjected too, she exclaimed!! It was NOT Meth by a long shot. When I watched this episode on Gilligans Island I was sure they would get spun, I mean it looked get on paper, but it don't appear to work, unless one of these there characters screwed things up, by not following Betty Crockers recipe book to a tee, but it looked straight forward, but it sure didn't go forward! Skipper put out a plea, PLEASE somebody help my LITTLE buddy Gilligan, he hates to a unsucessful Smurf ;-) Pyrex out P.S.-Chem Guy- What I had in mind was somethin along the lines of maybe like Gilligan writing up some reaction guidelines that he had observed hands-on exp, and then give his thoughts on what seemed to work the best most of the time, and then send you the material and then you could edit, add, or whatever you'd like to the material, maybe give the reason why it shoud or should be done a certain way etc. Basically you'd put the finishing touches on it, and then we could present it for informational purposes ONLY on the hive or Rhodium's board if it meets his standards. Gilligan had thought about a solo post, but in reality it would probably be more beneficial to bees if it was a co-op venture since Gilligan knows he ain't the shi*, when it comes to facts, he only knows what he has seen, and then with his limited I.Q. , well his guessing at things would just make things worse, but if he had a expert on the subject proof read the post, well it just might be presentable ;-) Pyrex out again |
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